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Failure Analysis Case Histories
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Fatigue Cracking
of Steam Line Expansion Bellow
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ENVIRONMENT:
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Oil Refinery |
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EQUIPMENT:
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Steam |
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MATERIAL: |
Type 304 Stainless Steel |
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SERVICE TIME: |
3 Years Active |
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FAILURE MODE:
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Fatigue Cracking |
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Summary
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Failure of the bellows occurred
first as a fatigue crack at the weld joining the lower end of the bellows to the
pipe. Failure then propagated as ductile tears perpendicular to the cracked
weld. Once the bellows opened up enough to relieve the internal pressure,
cracking continued to propagate as chloride stress corrosion cracks until the
bellows was removed from service.
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Background |
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The subject bellows was part of
an expansion joint assembly in a superheated steam line operating at 750°F. This assembly was oriented in a vertical position, and the failed bellows
was the upper of two bellows in the overall assembly. There was an internal
flow guide on the inside of this bellows in the form of a portion of straight
stainless steel tube welded to the pipe at the bottom edge of the bellows and
open at its top. The purpose of this flow guide was to minimize steam
turbulence inside the bellows.
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This tubular internal guide had
one or more drain holes drilled near its lower end to prevent steam condensate
from accumulating between the guide and the bellows. The drain holes were a
fraction of an inch above the joining circumferential weld, which meant that a
small amount of condensate could still accumulate there. Plant personnel were
concerned that such an accumulation might have somehow led to the failure of the
bellows.
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There was also an external
protective shield, in the form of a piece of steel pipe welded to an external
ring just above the bellows and open on its lower end. This shield was larger
than the bellows and stood out from it on all sides so as not to contact the
bellows directly. The question was also raised as to whether this shield might
have contributed to the failure.
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The bellows was made of Type
304 stainless steel and was in service for three years.
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Findings
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Visual examination revealed that
the bellows had cracked along the weld that had joined the bottom end of the
bellows to its mating pipe. This crack extended approximately half way around
the circumference of the bellows. The remainder of the circumference had been
cut with an abrasive disk to remove the bellows. It was not clear whether the
crack originally extended only about half way around the circumference, or
whether it had been longer but part of it was obliterated by the cutting
operation.
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When viewed under a low-power
microscope, the circumferential crack had a “woody” fracture surface typical of
fatigue failures of stainless steel welds. This is illustrated in Figure 1. No
clear initiation point for this crack was found, and no mechanical damage was
seen that might have caused high local stresses to initiate such a crack. |
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Figure 1. Portion of the
fracture surface showing the “woody” pattern typical of fatigue of stainless
steel welds. (27X original magnification)
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Figure 2. Crack originated at the circumferential fatigue
crack (lower right) and propagated toward the left in this view. Note that
this crack quickly changes to a plane approximately 45 degrees from the
metal surface. (6X original magnification) |
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Initiating from the
circumferential crack were several other cracks, mostly smaller in
magnitude than the circumferential crack and starting perpendicular to it.
These include:
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Crack Observation #1 |
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A long crack ran roughly perpendicular to the circumferential crack for a
distance of about six inches, and then itself became circumferential in nature
for a distance of roughly three inches. At this point, it turned and ran
roughly along the axis of the pipeline. |
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On close examination it was seen that this second crack, where it took off from
the circumferential crack, was on a plane approximately 45°
relative to the surfaces of the bellows. Unlike the woody appearance of
the first crack, this one had a smoother surface typical of simple tensile
failure. After traveling perpendicular to the circumferential crack for
about an inch, this second crack split into two cracks in a “Y” pattern.
One leg of this “Y” continued on while the other leg propagated only a short
distance., Figure 2.
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The last
inch or so of the crack went off at an angle. This last portion of the crack
showed a distinct branching pattern. Microscopic examination of this crack in a
plane cut through the bellows wall showed that the crack propagation in this
case was from the outside in. |
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Crack Observation #2 |
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A third crack, also starting perpendicular to the major circumferential
crack, was observed. This crack initially occurred on a 45°
plane as did the second crack, but, after traveling roughly two inches, made an
abrupt 90° turn in a circumferential
direction. Shortly thereafter it split into two cracks. One
continued in the circumferential direction and the other propagated in a
more axial direction. |
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Crack Observation #3 |
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Three
additional short cracks were observed. Two of these three cracks,
like the last inch of the second crack described in “1” above showed a more
wandering nature with much branching.
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Visual examination of the
various crack faces showed that the major circumferential crack was discolored
(oxidized), whereas the other cracks were less discolored and, in some cases,
had a bright metal surface. The oxidation of the primary crack was evident in
Figures 1.
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The last inch of the second crack (item 1
above) that included the wandering, branched characteristics, was cut out,
mounted, and examined at higher magnification. The branching nature
was apparent in Figure 53 In the higher magnification view in Figure 4
it was seen that the crack was transgranular. This branching,
transgranular pattern is typical of chloride stress corrosion cracking of
stainless steels. |
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The mounted specimen was placed
in the SEM and an EDS semi-quantitative microprobe analysis done at several
locations in and away from the crack. A summary of the analyses was compiled in
Table 1. |
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Figure 3. Magnified view of end portion of crack shown in Figure
3. (50X original magnification)
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Table 1.
EDS Analysis (WT%) |
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In crack |
Near crack |
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Iron |
55 |
68 |
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Chromium |
20 |
20 |
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Nickel |
2 |
9.2 |
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Silicon |
7 |
1.0 |
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Chloride |
14 |
-- |
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Material Testing |
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A sample of the
metal adjacent to the primary circumferential crack was cut and polished and microhardness measurements were made in the base metal, the weld metal, and at
the weld/base metal interface. In all cases the readings fell within the range
of 92-98 Rockwell B.
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Another sample was cut from the
bellows, mounted, and electrolytically etched with oxalic acid to look for
carbide precipitation along grain boundaries. The grain structure was normal
for this alloy and no grain boundary carbide precipitation was seen.
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Discussion |
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The “woody” appearance of the
circumferential crack is typical of intergranular fatigue of wrought stainless
steel or interdendritic fatigue of stainless weld metal. When such alloys are
exposed to elevated temperatures above about 1000°F, a second phase called “sigma” phase slowly forms along grain boundaries.
This metallic phase is extremely brittle and has been blamed for similar
failures of stainless steel components in the past. Sigma phase is also quite
hard, however, and its presence can usually be detected by making microhardness
measurements of the alloy. In this case there was no such apparent increase in
hardness, as evidenced by the very normal measurements obtained in and adjacent
to the fracture zone.
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One other known cause for
fatigue being intergranular is precipitation of a brittle carbide phase at the
grain boundaries resulting from what is called “sensitization” of the alloy due
to extended exposure to elevated temperatures. The 750°F operating temperature of this bellows is somewhat low for sensitization of
Type 304 stainless steel. Indeed, no such grain boundary precipitation was
found. This particular failure, therefore, was simply a result of high cyclic
stresses along the weld caused by vibration in the line. The edge of the
circumferential fillet weld in this case is an area of high localized stresses,
and is the area most likely to develop such fatigue cracks given cyclic loading
of the part.
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Corrosion fatigue is
perhaps a more accurate description of the failure. Corrosion fatigue simply
refers to mechanical fatigue that occurs in a medium somewhat more corrosive
than dry air. Steam certainly qualifies as such a medium, especially since
chloride was discovered in the crack.. To have corrosion
fatigue does not mean that there is visible corrosion of the metal. Rather, it
simply means that the fatigue crack develops more rapidly than it would have if
the part were only exposed to dry air. Corrosion fatigue usually cannot be
determined after the fact, as the crack morphology appears identical to other
mechanical fatigue. The only way to show that corrosion fatigue is a factor
would be to run controlled laboratory fatigue tests of the part in question in
both dry air and in the actual medium of exposure – steam in this case. The
extent to which failure occurs more rapidly in the non-air medium determines how
susceptible that part is to corrosion fatigue in the given environment. In this
case, the presence of steam is a given, and the role that it may have played in
accelerating this particular failure is academic.
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